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Synthesis of 6-Bromo-2-hydrazinylquinoline (3) The stirred suspension of compound 2 (13 g, 53.94 mmol, 1 equiv.) and hydrazine hydrate (16.8 mL, 80% in H 2 O, 82.86 mmol, 5 equiv.) was heated at 100 C for 16 h