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Statements Author contributions All authors listed have contributed equally and made a substantial, direct and intellectual contribution to the work, and approved it for publication

Rao CV, Asch AS, Carr DJJ, Yamada HY

At the indicated time points after adding formaldehyde (0, 10, 20, 40, 60, 120, 240 and 360 min), a sample was taken and diluted 1:50 in extraction solvent for LCMS measurements (concentration of compounds ~50 M) or 1:10 in water for GCMS-based detection of formaldehyde (highest concentration = 125 M)

18a, 18b, and 18c, respectively was then washed with DMF (10 times) and ethanol (10 times) and finally dried in vacuo