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1 H NMR (400 MHz, DMSO- d 6 ) 12.29 (d, J = 48.1 Hz, 1H), 11.05 (s, 1H), 7.817.66 (m, 2H), 7.56 (ddd, J = 5.9, 3.9, 2.2 Hz, 1H), 7.32 (d, J = 9.8 Hz, 1H), 6.726.59 (m, 1H), 5.05 (dd, J = 12.6, 5.3 Hz, 1H), 4.224.01 (m, 2H), 3.97 (dd, J = 12.0, 3.8 Hz, 2H), 3.75 (s, 1H), 3.64 (t, J = 6.1 Hz, 2H), 3.523.45 (m, 10H), 2.932.78 (m, 3H), 2.732.64 (m, 1H), 2.50 (dd, J = 23.7, 11.3 Hz, 3H), 1.99 (dd, J = 12.5, 6.9 Hz, 1H), 1.90 (d, J = 13.8 Hz, 1H), 1.67 (t, J = 43.3 Hz, 3H), 1.09 (t, J = 13.3 Hz, 9H)